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Question: SYNTHESIS OF CARBONATOTETRAAMMINECOBALT(III) NITRATE, [Co(NH3)4CO3]NO3 YIELS 42.97% ANDSYNTHESIS OF PENTAAMMINECHLOROCOBALT(III) CHLORIDE, [Co(NH3)5Cl]Cl2 YIELS 42.33% DISCUSS
The synthesis of both Carbonatotetraaminecobalt(III) nitrate and Pentaaminechlorocobalt(III) chloride have been performed and the yield percentages have been calculated as 42.97% and 42.33%, respectively. 1. Yield percentage: The yield percentage refers to the amount of desired product obtained from the chemical reaction compared to the theoretical maximum yield that could be produced. In this instance, the yield percentages for both substances fall below 50% which indicates that there are some losses during the synthesis process. 2. Possible reasons for low yields: a. Incomplete reactions: The reaction conditions might not have allowed the reaction to go to completion. This could involve issues with temperature, pressure and mixing. b. Loss during purification: A significant amount of product can often be lost during the purification process through side reactions and/or physical loss. c. Side reactions: These might have occurred where reactants or intermediate products form unwanted products, reducing the amount of final product. 3. Improvements: The synthesis process can potentially be improved by optimizing reaction conditions like temperature and pressure, improving purification techniques, or using excess of limiting reagents to drive the reaction to completion. 4. It's also worth taking into consideration that not all reactions can achieve 100% yields due to various practical limitations. However, comparing the yields for the two reactions could provide useful information, such as the efficiency of different synthetic routes or the stability of the different products. As always, remember to follow good lab practices, such as accurately measuring reactants, carefully controlling reaction conditions, and limiting loss of product during isolation and purification to maximize yield.
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